22D40 - Physico-chemical methods in surface characterization
Course specification | ||||
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Course title | Physico-chemical methods in surface characterization | |||
Acronym | 22D40 | |||
Study programme | Chemical Engineering,Metallurgical Enginering | |||
Module | ||||
Lecturer (for classes) | ||||
Lecturer/Associate (for practice) | ||||
Lecturer/Associate (for OTC) | ||||
ESPB | 6.0 | Status | ||
Condition | Облик условљености | |||
The goal | The course covers the physico-chemical basic for a range of instrumental methods/techniques for spectroscopic and microscopic surface characterisation. It discusses how these methods can be applied to gain specific knowledge about morphology, structure, the type of bonds and functional groups on surfaces, chemical and functional properties of surfaces. The student should master the knowlegde where these methods could be applied (biomaterials, polymers, ceramic and metal materials, in catalisys, nanomaterials, in protection, corrosion, tribology, pharmaceutical engineering....). | |||
The outcome | Student has acquired basic theoretical knowledge on different modern techniques applied in surface characterization. At the end of this course student will be able to describe the rande of instrumental methods/ techniques for analysing surfaces, what information these techniques provide and their weaknesses and limitations. Student will be able to chosse the appropriate method for characterization of a particular material, to evaluate results and easily learn how to work on particular instrument. | |||
Contents | ||||
Contents of lectures | • Introduction to surface analysis: surface sensitivity and surface specificity • High vacuum environment; Degrees of vacuum • Spectroscopic techniques in surface characterization: fundamentals and application • XPS – X-ray Photoelectron Spectroscopy • AES –Auger Electron Spectroscopy • UPS –Ultraviolet Photoelectron Spectroscopy • LEIS –Low energy ion scattering • LEED –Low Energy Electron Diffraction • TPD –Temperature Programmed Techniques • Scanning probe microscopy: fundamentals and application • AFM –atomic force microscopy • STM –scanning tunneling microscopy • Examples of different surface techniques in surface characterization | |||
Contents of exercises | ||||
Literature | ||||
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Number of hours per week during the semester/trimester/year | ||||
Lectures | Exercises | OTC | Study and Research | Other classes |
3 | ||||
Methods of teaching | Lectures, demonstration of AFM/STM, seminar, consultations | |||
Knowledge score (maximum points 100) | ||||
Pre obligations | Points | Final exam | Points | |
Activites during lectures | Test paper | |||
Practical lessons | Oral examination | 70 | ||
Projects | ||||
Colloquia | ||||
Seminars | 30 |